(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:1443004-99-6
Molecular Formula:C₂₈H₄₀N₂O₁₃S₂
Molecular Weight:676.763
Hs Code.:

Synonyms:(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 3 articles about (2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3-mercapto-N-(4-sulfamoylphenethyl)propanamide

: 10343-15-4,39698-55-0,54400-76-9,78730-32-2,119111-31-8,119111-32-9
Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-allyloxy-tetrahydro-pyran-4-yl ester

: 1443004-99-6
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With Bromotrichloromethane; bismuth(III) oxide; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Irradiation; Green chemistry;
DOI:10.1021/acs.orglett.5b03184

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 1443004-99-6
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 20 h / 0 - 20 °C / Inert atmosphere

2: 2,2'-azobis(isobutyronitrile) / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

With 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; In 1,4-dioxane; dichloromethane;
DOI:10.1039/c3cc42541j

Reference yield:

: bis[N-(4-sulfamoylphenethyl)]-3,3’-dithiodipropanamide

: 1443004-99-6
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-((3-oxo-3-((4-sulfamoylphenethyl)amino)propyl)thio)propoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: Multi-step reaction with 2 steps

1: diothiothreitol / N,N-dimethyl-formamide / 24 h / 20 °C

2: 2,2'-azobis(isobutyronitrile) / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

With 2,2'-azobis(isobutyronitrile); diothiothreitol; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42541j