N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

Base Information

Chemical Name:N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide
CAS No.:187996-42-5
Molecular Formula:C₃₉H₅₇NO₈S₂
Molecular Weight:732.015
Hs Code.:

Synonyms:N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

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Chemical Property of N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

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Technology Process of N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

There total 15 articles about N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 187996-35-6
2-Benzenesulfonylmethyl-3,4-dimethyl-5-propyl-furan

: 187996-41-4
N-{1-[2-(9-Bromo-nonyl)-5,5-dimethyl-[1,3]dioxan-2-yl]-2-hydroxy-ethyl}-benzenesulfonamide

: 187996-42-5
N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 0 ℃;
DOI:10.1016/S0040-4039(97)00074-9

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 187996-42-5
N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 7 steps

1: pTSA / CH₂Cl₂

2: 1.) Mg, 2.) n-BuLi / 1.) THF, 2.) THF, -78 deg C to r.t., 40 h

3: imidazole / CH₂Cl₂

4: 1.) acidic methanol, 2.) NBS, PPh₃ / 2.) CH₂Cl₂

5: TBAF / tetrahydrofuran

6: pTSA / benzene / Heating

7: 78 percent / NaHMDS / tetrahydrofuran / -78 - 0 °C

With 1H-imidazole; methanol; N-Bromosuccinimide; n-butyllithium; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; triphenylphosphine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1016/S0040-4039(97)00074-9

Reference yield:

: 55695-90-4
2-(9-bromononyloxy)tetrahydropyran

: 187996-42-5
N-(1-{2-[10-Benzenesulfonyl-10-(3,4-dimethyl-5-propyl-furan-2-yl)-decyl]-5,5-dimethyl-[1,3]dioxan-2-yl}-2-hydroxy-ethyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Mg, 2.) n-BuLi / 1.) THF, 2.) THF, -78 deg C to r.t., 40 h

2: imidazole / CH₂Cl₂

3: 1.) acidic methanol, 2.) NBS, PPh₃ / 2.) CH₂Cl₂

4: TBAF / tetrahydrofuran

5: pTSA / benzene / Heating

6: 78 percent / NaHMDS / tetrahydrofuran / -78 - 0 °C

With 1H-imidazole; methanol; N-Bromosuccinimide; n-butyllithium; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; triphenylphosphine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1016/S0040-4039(97)00074-9