5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Base Information

Chemical Name:5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer
CAS No.:106750-84-9
Molecular Formula:C₅₂H₄₀O₇
Molecular Weight:776.885
Hs Code.:

Synonyms:5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Suppliers and Price of 5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

There total 4 articles about 5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 106750-85-0
25-allyloxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

: 106750-84-9
5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Guidance literature:: With N,N-diethylaniline; for 2h; Inert atmosphere; Reflux;
DOI:10.1021/jo802714q

Reference yield:

: 157432-87-6,288302-11-4,288302-12-5,60705-62-6
5,11,17,23-tetra-t-butyl-25,26,27,28-tetrahydroxycalix-4-arene

: 106750-84-9
5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / phenol, AlCl₃ / toluene / 1 h / Ambient temperature

2: 71 percent / pyridine / 1) 0 deg C, 1 h 2) R_.T_., 1 h

3: 58 percent / NaH / tetrahydrofuran; dimethylformamide / 6 h / Heating

4: 62 percent / N,N-diethylaniline / 4 h / Heating

With aluminium trichloride; sodium hydride; N,N-diethylaniline; phenol; In tetrahydrofuran; pyridine; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4020(01)87580-3

Reference yield:

: 248590-47-8,74568-07-3
25,26,27,28-tetrakis(hydroxy)calix[4]arene

: 106750-84-9
5-allyl-25-hydroxy-26,27,28-tribenzoyloxycalix<4>arene 1,3-alternate conformer

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / pyridine / 1) 0 deg C, 1 h 2) R_.T_., 1 h

2: 58 percent / NaH / tetrahydrofuran; dimethylformamide / 6 h / Heating

3: 62 percent / N,N-diethylaniline / 4 h / Heating

With sodium hydride; N,N-diethylaniline; In tetrahydrofuran; pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)87580-3