benzyl N-(2-dimethylaminoethylmethyloxo-λ⁶-sulfanylidene)carbamate trifluoroacetic acid

Base Information

• Chemical Name: benzyl N-(2-dimethylaminoethylmethyloxo-λ⁶-sulfanylidene)carbamate trifluoroacetic acid
• CAS No.: 1609963-60-1
• Molecular Formula: C₂HF₃O₂*C₁₃H₂₀N₂O₃S
• Molecular Weight: 398.403
• Mol file: 1609963-60-1.mol

Synonyms:benzyl N-(2-dimethylaminoethylmethyloxo-λ⁶-sulfanylidene)carbamate trifluoroacetic acid

Chemical Property of benzyl N-(2-dimethylaminoethylmethyloxo-λ⁶-sulfanylidene)carbamate trifluoroacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of benzyl N-(2-dimethylaminoethylmethyloxo-λ⁶-sulfanylidene)carbamate trifluoroacetic acid

There total 2 articles about benzyl N-(2-dimethylaminoethylmethyloxo-λ⁶-sulfanylidene)carbamate trifluoroacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzyl (dimethyl(oxo)-λ6-sulfaneylidene)carbamate (62995-07-7) + eschenmoser's salt (33797-51-2) → benzyl N-(2-dimethylaminoethylmethyloxo-λ6-sulfanylidene)carbamate trifluoroacetic acid (1609963-60-1)

Guidance literature:

Benzyl (dimethyl(oxo)-λ⁶-sulfaneylidene)carbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -10 ℃; for 1h;

eschenmoser's salt; In tetrahydrofuran; hexane; at 0 - 20 ℃;

Reference yield:

Benzyl (dimethyl(oxo)-λ6-sulfaneylidene)carbamate (62995-07-7) + eschenmoser's salt (33797-51-2) + trifluoroacetic acid (76-05-1) → benzyl N-(2-dimethylaminoethylmethyloxo-λ6-sulfanylidene)carbamate trifluoroacetic acid (1609963-60-1)

Guidance literature:

Benzyl (dimethyl(oxo)-λ⁶-sulfaneylidene)carbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

eschenmoser's salt; In tetrahydrofuran; hexane; at -10 - 20 ℃;

trifluoroacetic acid;

upstream raw materials:

Benzyl (dimethyl(oxo)-λ⁶-sulfaneylidene)carbamate

eschenmoser's salt

trifluoroacetic acid