5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

Base Information

Chemical Name:5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol
CAS No.:1355364-33-8
Molecular Formula:C₃₈H₄₄N₂O₃
Molecular Weight:576.779
Hs Code.:

Synonyms:5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

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Chemical Property of 5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

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Technology Process of 5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

There total 5 articles about 5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355364-32-7
5-(4-(4-(4-(aminomethyl)phenoxy)butoxy)benzylamino)pentan-1-ol

: 642-31-9
9-anthracene aldehyde

: 1355364-33-8
5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

Guidance literature:: 5-(4-(4-(4-(aminomethyl)phenoxy)butoxy)benzylamino)pentan-1-ol; 9-anthracene aldehyde; In ethanol; for 24h; Reflux; Inert atmosphere;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja2107096

Reference yield:

: 767-00-0
4-cyanophenol

: 1355364-33-8
5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 48 h / Reflux; Inert atmosphere

2.1: ethanol / 24 h / Reflux; Inert atmosphere

2.2: 24 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 0 °C / Reflux

4.1: ethanol / 24 h / Reflux; Inert atmosphere

4.2: 24 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ja2107096

Reference yield:

: 1355364-30-5
4-(4-(4-cyanophenoxy)butoxy)benzaldehyde

: 1355364-33-8
5-(4-(4-(4-(((9-anthracenyl)methylamino)methyl)phenoxy)butoxy)benzylamino)pentan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 24 h / Reflux; Inert atmosphere

1.2: 24 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 0 °C / Reflux

3.1: ethanol / 24 h / Reflux; Inert atmosphere

3.2: 24 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; In tetrahydrofuran; ethanol;
DOI:10.1021/ja2107096