methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside
CAS No.:115520-89-3
Molecular Formula:C₃₀H₃₆O₈
Molecular Weight:524.611
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

Chemical Property:

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Technology Process of methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

There total 6 articles about methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 125288-00-8
methyl (methyl-2,3,4-tri-O-benzyl-l-threo-α-D-manno-octopyranoside)uronate

: 115520-89-3
methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 15h; Inert atmosphere;
DOI:10.1002/chem.201100396

Reference yield:

: 34212-64-1,641635-63-4
methyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 115520-89-3
methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) O₂ / 1.) Swern oxidation; 2.) benzene, reflux, 90 min

2: N-methylmorpholine N-oxide monohydrate, osmium tetraoxide (OsO₄) / acetone; H₂O / Ambient temperature

With osmium(VIII) oxide; oxygen; 4-methylmorpholine N-oxide; In water; acetone;
DOI:10.1016/0008-6215(88)84106-5

Reference yield:

: 115520-88-2
methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-oct-6(E)-eno-α-D-manno-1,5-pyranoside

: 115520-89-3
methyl 2,3,4-tri-O-benzyl-β-L-threo-D-manno-octopyranoside

: 115520-90-6
methyl 2,3,4-tri-O-benzyl-α-D-threo-D-manno-octopyranoside

Guidance literature:: With water; 4-methylmorpholine N-oxide; osmium(VIII) oxide; In acetone; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;