3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

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Chemical Name:3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate
CAS No.:1340480-26-3
Molecular Formula:C₂HF₃O₂*C₂₇H₂₄ClF₃N₆O₃
Molecular Weight:686.998
Hs Code.:

3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

Synonyms:3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

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Chemical Property of 3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

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Technology Process of 3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

There total 2 articles about 3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1155846-67-5
3-chloro-5-{[2-oxo-1-(1H-pyrazolo[3,4-b]pyridin-3-ylmethyl)-4-(trifluoromethyl)-1,2-dihydropyridin-3-yl]oxy}benzonitrile

: 95037-43-7
3-dimethylamino-2,2-dimethyl-propionyl chloride ; hydrochloride

: 76-05-1
trifluoroacetic acid

: 1340480-26-3
3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

Guidance literature:: 3-chloro-5-{[2-oxo-1-(1H-pyrazolo[3,4-b]pyridin-3-ylmethyl)-4-(trifluoromethyl)-1,2-dihydropyridin-3-yl]oxy}benzonitrile; 3-dimethylamino-2,2-dimethyl-propionyl chloride ; hydrochloride; With pyridine; dmap; at 80 ℃; for 2h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 1615-10-7
3-dimethylamino-2,2-dimethyl-propionic acid ; hydrochloride

: 1340480-26-3
3-(3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)-N,N,2,2-tetramethyl-3-oxopropan-1-aminium trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 1 h

2: dmap; pyridine / 2 h / 80 °C

With pyridine; dmap; thionyl chloride;