(E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

Base Information

Chemical Name:(E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride
CAS No.:1579956-06-1
Molecular Formula:C₁₉H₁₉NO₄*ClH
Molecular Weight:361.825
Hs Code.:

Synonyms:(E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

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Chemical Property of (E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

Chemical Property:

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Technology Process of (E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

There total 3 articles about (E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1579956-07-2
(E)-cinnamyl 3-(3,4-bis(methoxymethoxy)phenyl)-2-((tert-butoxycarbonylamino)methyl)acrylate

: 1579956-06-1
(E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

Guidance literature:: With hydrogenchloride; water; In methanol; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2014.01.049

Reference yield:

: ethyl 3-(3,4-bis(methoxymethoxy)phenyl)-2-((tert-butoxycarbonylamino)methyl)acrylate

: 1579956-06-1
(E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / methanol; water / 12 h / 20 °C

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 20 °C

3: water; hydrogenchloride / methanol / 48 h / 20 °C

With hydrogenchloride; dmap; water; dicyclohexyl-carbodiimide; lithium hydroxide; In methanol; dichloromethane; water; 2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.ejmech.2014.01.049

Reference yield:

: 1446141-02-1
(E)-3-(3,4-bis(methoxymethoxy)phenyl)-2-((tert-butoxycarbonylamino)methyl)acrylic acid

: 1579956-06-1
(E)-2-(cinnamyloxycarbonyl)-3-(3,4-dihydroxyphenyl)prop-2-en-1-ammonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 20 °C

2: water; hydrogenchloride / methanol / 48 h / 20 °C

With hydrogenchloride; dmap; water; dicyclohexyl-carbodiimide; In methanol; dichloromethane; 1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.ejmech.2014.01.049