2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran

Base Information

• Chemical Name: 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran
• CAS No.: 128753-98-0
• Molecular Formula: C₁₉H₁₉NO₅
• Molecular Weight: 341.364

Synonyms:2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran

Chemical Property of 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran

There total 3 articles about 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran (128753-78-6) → 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran (128753-98-0)

Guidance literature:

With oxygen; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; at -20 ℃; for 6h; Irradiation;

Reference yield:

2-(hydroxymethyl)-3-methylbenzofuran (55581-62-9) → 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran (128753-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / Ambient temperature

2: 25 percent / oxygen / tetraphenylporphine / CH₂Cl₂ / 6 h / -20 °C / Irradiation

With dmap; oxygen; dicyclohexyl-carbodiimide; 5,15,10,20-tetraphenylporphyrin; In dichloromethane;

Reference yield:

p-N,N-dimethylaminobenzoic acid (619-84-1) → 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran (128753-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 3 h / Ambient temperature

2: 25 percent / oxygen / tetraphenylporphine / CH₂Cl₂ / 6 h / -20 °C / Irradiation

With dmap; oxygen; dicyclohexyl-carbodiimide; 5,15,10,20-tetraphenylporphyrin; In dichloromethane;

upstream raw materials:

2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran

2-(hydroxymethyl)-3-methylbenzofuran

p-N,N-dimethylaminobenzoic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 128753-98-0 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran

Send

Send

Metric Ton KG G Pound L ML

Send

Send