tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

Base Information

Chemical Name:tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate
CAS No.:1261254-08-3
Molecular Formula:C₂₃H₃₆N₂O₂
Molecular Weight:372.551
Hs Code.:

Synonyms:tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

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Chemical Property of tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

There total 5 articles about tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31252-42-3
4-benzylpyperidine

: 347185-69-7
((1S,3R)-3-(tert-butoxycarbonylamino)cyclopentyl)methyl 4-methylbenzenesulfonate

: 1261254-08-3
tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 6h;

Reference yield:

: 153011-43-9,172720-97-7
(1S,cis)-tert-butyl N-[4-(hydroxymethyl)-2-cyclopenten-1-yl]carbamate

: 1261254-08-3
tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

2: triethylamine / dichloromethane / 6 h / 20 °C

3: potassium carbonate / dichloromethane / 6 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium 10% on activated carbon; In ethanol; dichloromethane;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1261254-08-3
tert-butyl (1R,3S)-3-((4-benzylpiperidin-1-yl)methyl)cyclopentylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / tetrahydrofuran / 0.17 h / 0 - 20 °C

1.2: 12 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

3.1: triethylamine / dichloromethane / 6 h / 20 °C

4.1: potassium carbonate / dichloromethane / 6 h / 20 °C

With hydrogen; sodium carbonate; potassium carbonate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;