N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

Base Information

Chemical Name:N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide
CAS No.:1443542-61-7
Molecular Formula:C₁₇H₁₄ClN₃S
Molecular Weight:327.837
Hs Code.:

Synonyms:N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

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Chemical Property of N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

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Technology Process of N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

There total 1 articles about N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98546-51-1
(4-thiomethoxyphenyl)boronic acid

: 171774-38-2
N-(3-bromo-5-chloropyridin-2-yl)pyridin-1-ium-1-aminide

: 1443542-61-7
N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; toluene; for 12h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.05.065

Reference yield: 70.0%

: 1443542-61-7
N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

: 217090-19-2
5-chloro-3-(4-methylthiophenyl)-2-pyridinamine

Guidance literature:: With acetic acid; zinc; at 20 ℃; for 29h;
DOI:10.1016/j.tet.2013.05.065

Reference yield:

: 1443542-61-7
N-[5-chloro-3-(4-methylthiophenyl)pyridin-2-yl]pyridin-1-ium-1-aminide

: 1443542-78-6
5-chloro-3-(4-methylsulfinylphenyl)-2(1H)-pyridinone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; zinc / 29 h / 20 °C

2: sodium nitrite; sulfuric acid; pyridine / water / 2 h / 0 °C

With pyridine; sulfuric acid; acetic acid; zinc; sodium nitrite; In water;
DOI:10.1016/j.tet.2013.05.065