(+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

Base Information

Chemical Name:(+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester
CAS No.:911437-77-9
Molecular Formula:C₂₃H₂₉NO₅
Molecular Weight:399.487
Hs Code.:

Synonyms:(+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

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Chemical Property of (+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

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Technology Process of (+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

There total 14 articles about (+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1214892-41-7
C₁₇H₂₄O₆

: 62-53-3
aniline

: 911437-77-9
(+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 0 - 20 ℃; for 48h;
DOI:10.1021/ml100028g

Reference yield: 39.0%

: 911437-74-6
(+/-)-7-hydroxy-7-phenylcarbamoylheptanoic acid methyl ester

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 911437-77-9
(+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/j.bmcl.2007.09.014

Reference yield:

: 5-(2,2-dimethyl-5-oxo-[1,3]dioxolan-4-yl)-pentanoyl chloride

: 911437-77-9
(+/-)-7-(4-methoxybenzyloxy)-7-phenylcarbamoyl heptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether; CH₂Cl₂ / -5 - 20 °C

2: 99 percent / AgOBz; Et₃N / -25 - 20 °C

3: 1,2,4-triazole / CH₂Cl₂ / 0 - 20 °C

4: BF₃*Et₂O / CH₂Cl₂; diethyl ether

With 1,2,4-Triazole; boron trifluoride diethyl etherate; silver benzoate; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1016/j.bmcl.2006.06.090