1,1'-(benzylimino)dipropan-2-one dioxime

Base Information

• Chemical Name: 1,1'-(benzylimino)dipropan-2-one dioxime
• CAS No.: 1319736-30-5
• Molecular Formula: C₁₃H₁₉N₃O₂
• Molecular Weight: 249.313
• Mol file: 1319736-30-5.mol

Synonyms:1,1'-(benzylimino)dipropan-2-one dioxime

Chemical Property of 1,1'-(benzylimino)dipropan-2-one dioxime

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1'-(benzylimino)dipropan-2-one dioxime

There total 2 articles about 1,1'-(benzylimino)dipropan-2-one dioxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N,N-bis(trimethylsilyloxy)-1-propen-2-amine (102588-22-7) + benzylamine (100-46-9) → 1,1'-(benzylimino)dipropan-2-one dioxime (1319736-30-5)

Guidance literature:

N,N-bis(trimethylsilyloxy)-1-propen-2-amine; benzylamine; In dichloromethane; at 20 ℃; for 24h;

With methanol; In dichloromethane; for 0.5h;

DOI:10.1016/j.poly.2014.01.003

Reference yield:

N,N-bis(trimethylsilyloxy)-1-propen-2-amine (102588-22-7) + benzylamine (100-46-9) → 1,1'-(benzylimino)dipropan-2-one dioxime + 1,1'-(benzylimino)dipropan-2-one dioxime (1319736-30-5)

Guidance literature:

N,N-bis(trimethylsilyloxy)-1-propen-2-amine; benzylamine; In dichloromethane; at 20 ℃; for 12h;

With methanol; In dichloromethane; at 20 ℃; for 5h; optical yield given as %de;

DOI:10.1055/s-0030-1259995

upstream raw materials:

N,N-bis(trimethylsilyloxy)-1-propen-2-amine

benzylamine

Refernces

• 1、 Semakin, Artem N.,Sukhorukov, Alexey Yu.,Ioffe, Sema L.,Tartakovsky, Vladimir A.. "A general procedure for the synthesis of unsymmetrically substituted tris(β-oximinoalkyl)amines". experimental part. p. 1403 - 1412. Retrieved 2011/06/19.