4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester

Base Information

Chemical Name:4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester
CAS No.:82825-38-5
Molecular Formula:C₂₇H₁₄Cl₁₄NO₃
Molecular Weight:896.755
Hs Code.:

Synonyms:4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester

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Chemical Property of 4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester

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Technology Process of 4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester

There total 2 articles about 4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 13404-22-3
tert-butyl L-alaninate hydrochloride

: 77225-19-5
Tetradecachloro-4-(chlorocarbonyl)triphenylmethyl Radical

: 82825-38-5
4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester

Guidance literature:: With triethylamine; In water; benzene; for 24h; Ambient temperature;
DOI:10.1021/jo00169a021

Reference yield:

: 77212-86-3
(tetradecachloro-4-carboxytriphenyl)methyl radical

: 82825-38-5
4-(Alaninocarbonyl)tetradecachlorotriphenylmethyl radical tert butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / SOCl₂ / 24 h / Heating; other reagent: PCl₅ and POCl₃

2: 97 percent / triethylamine / benzene; H₂O / 24 h / Ambient temperature

With thionyl chloride; triethylamine; In water; benzene;
DOI:10.1021/jo00169a021