methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

Base Information

Chemical Name:methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)
CAS No.:1428238-26-9
Molecular Formula:C₆₅H₇₄O₁₈
Molecular Weight:1143.29
Hs Code.:

Synonyms:methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

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Chemical Property of methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

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Technology Process of methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

There total 3 articles about methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₆₇H₇₆O₁₉

: 1428238-26-9
methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

Guidance literature:: With potassium carbonate; In methanol; for 4h;

Reference yield: 59.0%

: methyl [2,3,6-tri-O-benzyl-4-O-(2-naphthyl)methyl-α-D-glucopyranosyl]-(1→4)-[methyl (2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

: 1428238-26-9
methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 0.5h;
DOI:10.3390/molecules21111497

Reference yield: 22.0%

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: methyl [2,3,6-tri-O-benzyl-4-O-(4-methoxybenzyl)-α,β-D-glucopyranosyl]-(1→4)-2-O-acetyl-3-O-methyl-1-O-trichloroacetimidoyl-α,β-L-idopyranosyluronate

: methyl (2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-(1→4)-(methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 1428238-26-9
methyl [2,3,6-tri-O-benzyl-α-D-glucopyranosyl]-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-(2,3,6-tri-O-benzyl-α-D-glucopyranoside)

Guidance literature:: methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside; methyl [2,3,6-tri-O-benzyl-4-O-(4-methoxybenzyl)-α,β-D-glucopyranosyl]-(1→4)-2-O-acetyl-3-O-methyl-1-O-trichloroacetimidoyl-α,β-L-idopyranosyluronate; In dichloromethane; at -20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; for 2h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.076