C₂₁H₂₄Cl₂O₃

Base Information

Chemical Name:C₂₁H₂₄Cl₂O₃
CAS No.:1619930-27-6
Molecular Formula:C₂₁H₂₄Cl₂O₃
Molecular Weight:395.326
Hs Code.:

C<sub>21</sub>H<sub>24</sub>Cl<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₁H₂₄Cl₂O₃

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Chemical Property of C₂₁H₂₄Cl₂O₃

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Technology Process of C₂₁H₂₄Cl₂O₃

There total 4 articles about C₂₁H₂₄Cl₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1619930-25-4
C₂₁H₂₆Cl₂O₃

: 1619930-27-6
C₂₁H₂₄Cl₂O₃

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1002/anie.201403542

Reference yield:

: 137819-50-2
(3R,4R)-1-(benzyloxy)-4-methylhex-5-en-3-ol

: 1619930-27-6
C₂₁H₂₄Cl₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

1.2: 0 - 20 °C

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 8 h / 0 - 20 °C

2.2: 1 h / Reflux

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

With sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/anie.201403542

Reference yield:

: 1619930-23-2
C₂₁H₂₄Cl₂O₂

: 1619930-27-6
C₂₁H₂₄Cl₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 8 h / 0 - 20 °C

1.2: 1 h / Reflux

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

With sodium hydrogencarbonate; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201403542