benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

Base Information

Chemical Name:benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate
CAS No.:911228-45-0
Molecular Formula:C₃₃H₃₆N₂O₃
Molecular Weight:508.66
Hs Code.:

Synonyms:benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

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Chemical Property of benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

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Technology Process of benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

There total 1 articles about benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.9%

: 911228-44-9
C₂₃H₂₂F₃NO₅S

: 389621-80-1
4-(N,N-diethylaminocarbonyl)phenylboronic acid

: 911228-45-0
benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

Guidance literature:: With sodium carbonate; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; Heating / reflux;

Reference yield: 100.0%

: 911228-45-0
benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

: C₂₅H₃₂N₂O

Guidance literature:: benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate; With hydrogen; palladium 10% on activated carbon; In methanol; dichloromethane; at 20 ℃; for 48h;

With hydrogenchloride; In diethyl ether; dichloromethane; at 20 ℃; for 1h;

Reference yield: 93.0%

: 911228-45-0
benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate

: N,N-diethyl-4-(1H-spiro[naphthalene-2,4-piperidine]-4-yl)benzamide hydrochloride

Guidance literature:: benzyl 4-(4-(diethylcarbamoyl)phenyl)-1H-spiro[naphthalene-2,4-piperidine]-1'-carboxylate; With trimethylsilyl iodide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In diethyl ether; dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2009.04.094