benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

Base Information

Chemical Name:benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate
CAS No.:165689-76-9
Molecular Formula:C₅₃H₈₆O₁₃Si
Molecular Weight:959.344
Hs Code.:

Synonyms:benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

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Chemical Property of benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

There total 76 articles about benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 159153-49-8
(S)-2-{(2S,5R)-5-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-propyl]-tetrahydro-furan-2-yl}-propionic acid (S)-2-[(2S,5R)-5-((R)-1-benzyloxycarbonyl-ethyl)-tetrahydro-furan-2-yl]-1-methyl-ethyl ester

: 165689-76-9
benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / hydrogen / Pd/C / tetrahydrofuran / 5 h / 20 °C

2: 81 percent / 2,4,6-trichlorobenzoyl chloride; DMAP / CH₂Cl₂ / 47 h / 20 °C

With dmap; 2,4,6-trichlorobenzoyl chloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0609661

Reference yield:

: 159153-48-7
(S)-2-((2S,5R)-5-((R)-2-(tert-butyldimethylsiloxy)propyl)tetrahydrofuran-2-yl)propanoic acid

: 165689-76-9
benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / DCC; DMAP / CH₂Cl₂ / 20 h / 20 °C

2: 99 percent / hydrogen / Pd/C / tetrahydrofuran / 5 h / 20 °C

3: 81 percent / 2,4,6-trichlorobenzoyl chloride; DMAP / CH₂Cl₂ / 47 h / 20 °C

With dmap; 2,4,6-trichlorobenzoyl chloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0609661

Reference yield:

: 16221-10-6
(+)-(2S,3S,6R,8R)-epi-Nonactic acid

: 165689-76-9
benzyl 8-tert-butyldimethylsilyl-(+)-nonactyl-(-)-nonactyl-(+)-nonactyl-(-)-nonactate

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / NaH / hexane; dimethylformamide / 0.17 h

2: 80 percent / DCC; DMAP / CH₂Cl₂ / 20 h / 20 °C

3: 99 percent / hydrogen / Pd/C / tetrahydrofuran / 5 h / 20 °C

4: 81 percent / 2,4,6-trichlorobenzoyl chloride; DMAP / CH₂Cl₂ / 47 h / 20 °C

With dmap; 2,4,6-trichlorobenzoyl chloride; hydrogen; sodium hydride; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0609661