(S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

Base Information

Chemical Name:(S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide
CAS No.:910910-05-3
Molecular Formula:C₁₃H₂₅NOS
Molecular Weight:243.414
Hs Code.:

Synonyms:(S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

Suppliers and Price of (S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

Chemical Property:

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Technology Process of (S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

There total 3 articles about (S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910910-21-3
4-methyl-cyclohexanecarboxylic acid methoxy-methyl-amide

: 910910-05-3
(S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / 2 h / cooling

2: 0.952 g / Ti(OEt)4 / tetrahydrofuran / Heating

With titanium(IV) tetraethanolate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo061160h

Reference yield:

: 4331-54-8
4-methylcyclohexanecarboxylic acid

: 910910-05-3
(S)-(+)-N-[1-(cis-4-methyl-cyclohexyl)ethylidene]-2-methyl-2-propanesulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / 1-hydroxybenzotriazole; i-Pr₂EtN; N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 20 h

2: tetrahydrofuran; diethyl ether / 2 h / cooling

3: 0.952 g / Ti(OEt)4 / tetrahydrofuran / Heating

With titanium(IV) tetraethanolate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo061160h