5-(4-fluorophenoxy)-2-methylaminobenzoic acid

Base Information

Chemical Name:5-(4-fluorophenoxy)-2-methylaminobenzoic acid
CAS No.:1336910-83-8
Molecular Formula:C₁₄H₁₂FNO₃
Molecular Weight:261.253
Hs Code.:

Synonyms:5-(4-fluorophenoxy)-2-methylaminobenzoic acid

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Chemical Property of 5-(4-fluorophenoxy)-2-methylaminobenzoic acid

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Technology Process of 5-(4-fluorophenoxy)-2-methylaminobenzoic acid

There total 4 articles about 5-(4-fluorophenoxy)-2-methylaminobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1336910-82-7
5-(4-fluorophenoxy)-2-methylaminobenzoic acid methyl ester

: 1336910-83-8
5-(4-fluorophenoxy)-2-methylaminobenzoic acid

Guidance literature:: 5-(4-fluorophenoxy)-2-methylaminobenzoic acid methyl ester; With sodium hydroxide; In methanol; at 80 ℃; for 2h;

With hydrogenchloride; In water; pH=~ 6;

Reference yield:

: 371-41-5
4-Fluorophenol

: 1336910-83-8
5-(4-fluorophenoxy)-2-methylaminobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 1.5 h

2.1: hydrogen / palladium on activated charcoal / methanol / 20 °C / 760.05 Torr

3.1: N-ethyl-N,N-diisopropylamine / 1,1-dichloroethane; water / 0.08 h

3.2: 40 h

4.1: sodium hydroxide / methanol / 2 h / 80 °C

4.2: pH ~ 6

With hydrogen; N-ethyl-N,N-diisopropylamine; sodium hydroxide; palladium on activated charcoal; In methanol; 1,1-dichloroethane; water; dimethyl sulfoxide;

Reference yield:

: 1055974-04-3
5-(4-fluorophenoxy)-2-nitrobenzoic acid methyl ester

: 1336910-83-8
5-(4-fluorophenoxy)-2-methylaminobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium on activated charcoal / methanol / 20 °C / 760.05 Torr

2.1: N-ethyl-N,N-diisopropylamine / 1,1-dichloroethane; water / 0.08 h

2.2: 40 h

3.1: sodium hydroxide / methanol / 2 h / 80 °C

3.2: pH ~ 6

With hydrogen; N-ethyl-N,N-diisopropylamine; sodium hydroxide; palladium on activated charcoal; In methanol; 1,1-dichloroethane; water;