HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

Base Information

Chemical Name:HCCC₆H₄CHCHC₆H₄N(C₆H₅)2
CAS No.:1083095-50-4
Molecular Formula:C₂₈H₂₁N
Molecular Weight:371.481
Hs Code.:

HCCC<sub>6</sub>H<sub>4</sub>CHCHC<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>5</sub>)2

Synonyms:HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

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Chemical Property of HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

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Technology Process of HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

There total 6 articles about HCCC₆H₄CHCHC₆H₄N(C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: C₃₁H₂₇NO

: 1083095-50-4
HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

Guidance literature:: With potassium hydroxide; In isopropyl alcohol; Reflux;
DOI:10.1021/ma401085q

Reference yield:

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 1083095-50-4
HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / Reflux

2: potassium tert-butylate / tetrahydrofuran / Reflux

3: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine / toluene / Reflux

4: potassium hydroxide / isopropyl alcohol / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; isopropyl alcohol; toluene; 2: |Horner-Wadsworth-Emmons Olefination / 3: |Sonogashira Cross-Coupling;
DOI:10.1021/ma401085q

Reference yield:

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 1083095-50-4
HCCC₆H₄CHCHC₆H₄N(C₆H₅)2

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / tetrahydrofuran / Reflux

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine / toluene / Reflux

3: potassium hydroxide / isopropyl alcohol / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; isopropyl alcohol; toluene; 1: |Horner-Wadsworth-Emmons Olefination / 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ma401085q