[2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

Base Information

Chemical Name:[2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid
CAS No.:175447-66-2
Molecular Formula:C₁₈H₂₆O₁₀
Molecular Weight:402.398
Hs Code.:

Synonyms:[2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

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Chemical Property of [2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

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Technology Process of [2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

There total 1 articles about [2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35648-87-4
1,4-bis[2-(2-hydroxyethoxy)ethoxy]benzene

: 79-11-8
chloroacetic acid

: 175447-66-2
[2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

Guidance literature:: With potassium tert-butylate; Yield given. Multistep reaction; 1.) t-BuOH, reflux, 1 h, 2.) t-BuOH, reflux, 48 h;
DOI:10.1055/s-1996-4319

Reference yield: 100.0%

: 175447-66-2
[2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

: 175732-70-4
[2-(2-{4-[2-(2-Chlorocarbonylmethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In benzene; for 16h; Ambient temperature;
DOI:10.1055/s-1996-4319

Reference yield:

: 175447-66-2
[2-(2-{4-[2-(2-Carboxymethoxy-ethoxy)-ethoxy]-phenoxy}-ethoxy)-ethoxy]-acetic acid

: C₄₈H₆₂N₄O₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / (COCl)2, DMF / benzene / 16 h / Ambient temperature

2: 87 percent / Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

3: 50 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

With lithium aluminium tetrahydride; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1055/s-1996-4319