5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

Base Information

Chemical Name:5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid
CAS No.:1428441-18-2
Molecular Formula:C₁₅H₁₉N₃O₄
Molecular Weight:305.334
Hs Code.:

Synonyms:5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

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Chemical Property of 5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

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Technology Process of 5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

There total 6 articles about 5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1428441-17-1
5-acetamido-4-azido-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

: 1428441-18-2
5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

Guidance literature:: With hydrogen; In methanol; at 20 ℃; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/jm301892f

Reference yield:

: 62-53-3
aniline

: 1428441-18-2
5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / methanol / Inert atmosphere

2: sodium cyanoborohydride / Inert atmosphere

3: lithium hydroxide / methanol / 1 h / 20 °C / Inert atmosphere

4: hydrogen / methanol / 20 °C / 760.05 Torr / Inert atmosphere

With hydrogen; sodium cyanoborohydride; acetic acid; lithium hydroxide; In methanol;
DOI:10.1021/jm301892f

Reference yield:

: C₁₆H₁₉N₅O₄

: 1428441-18-2
5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-6-((phenylamino)methyl)-L-gluco-hex-2-enonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / methanol / 1 h / 20 °C / Inert atmosphere

2: hydrogen / methanol / 20 °C / 760.05 Torr / Inert atmosphere

With hydrogen; lithium hydroxide; In methanol;
DOI:10.1021/jm301892f