methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate

Base Information

• Chemical Name: methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate
• CAS No.: 1146629-58-4
• Molecular Formula: C₃₄H₃₅I₂N₉O₆
• Molecular Weight: 919.518

Synonyms:methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate

Chemical Property of methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate

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Technology Process of methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate

There total 1 articles about methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

3,5-diiodo-4-(2-methyl-1H-5-imidazolyl)benzoic acid (1146629-50-6) + C23H29N7O5 → methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate (1146629-58-4)

Guidance literature:

With triethylamine; dicyclohexyl-carbodiimide; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 24h;

DOI:10.3797/scipharm.0803-04

Reference yield: 90.0%

methyl 1-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophanate (1146629-58-4) → N-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophane (1146629-62-0)

Guidance literature:

With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.3797/scipharm.0803-04

upstream raw materials:

3,5-diiodo-4-(2-methyl-1H-5-imidazolyl)benzoic acid

Downstream raw materials:

N-[3,5-diiodo-4-(2-methyl-1H-imidazol-5-yl)benzoyl]glycyl-L-histidyl-L-alanyl-L-tryptophane

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