methyl 2,5-dioxo-3,5-diphenylpentanoate

Base Information

Chemical Name:methyl 2,5-dioxo-3,5-diphenylpentanoate
CAS No.:1292310-23-6
Molecular Formula:C₁₈H₁₆O₄
Molecular Weight:296.323
Hs Code.:

Synonyms:methyl 2,5-dioxo-3,5-diphenylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,5-dioxo-3,5-diphenylpentanoate

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Technology Process of methyl 2,5-dioxo-3,5-diphenylpentanoate

There total 3 articles about methyl 2,5-dioxo-3,5-diphenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 95276-54-3,112697-96-8,112697-98-0
cyano-2 oxo-5 diphenyl-3,5 pentanoate de methyle

: 1292310-23-6
methyl 2,5-dioxo-3,5-diphenylpentanoate

Guidance literature:: With iodine; In ethanol; at 50 ℃; for 8h; Green chemistry;
DOI:10.1055/s-0040-1707996

Reference yield: 79.0%

: 103594-31-6
methyl 2-acetyl-5-oxo-3,5-diphenylpentanoate

: 1292310-23-6
methyl 2,5-dioxo-3,5-diphenylpentanoate

Guidance literature:: With copper(II) nitrate trihydrate; oxygen; In acetonitrile; at 20 ℃; for 20h; under 3345.86 Torr; Air atmosphere;
DOI:10.1021/ol200649u

Reference yield:

: 94-41-7
benzalacetophenone

: 1292310-23-6
methyl 2,5-dioxo-3,5-diphenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium perchlorate; triethylamine / 0.17 h / 20 °C

2: copper(l) iodide; oxygen / acetonitrile / 3 h / 25 °C

With copper(l) iodide; oxygen; lithium perchlorate; triethylamine; In acetonitrile; 1: Michael condensation;
DOI:10.1002/adsc.201100431