Technology Process of C14H18BrNO3
There total 4 articles about C14H18BrNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; ammonium acetate; water;
In
acetone;
at -78 - 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/jo2026228
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium azide / water; acetone / 1 h / 0 °C / Inert atmosphere
1.2: Molecular sieve; atmospheric pressure short-path distillation; Inert atmosphere
2.1: ozone; Sudan III / dichloromethane / -78 °C
2.2: -78 °C
2.3: Reflux
3.1: N-Bromosuccinimide; ammonium acetate; water / acetone / 3 h / -78 - 20 °C / Inert atmosphere
With
N-Bromosuccinimide; sodium azide; ammonium acetate; water; ozone; Sudan III;
In
dichloromethane; water; acetone;
DOI:10.1021/jo2026228
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: silver nitrate; sodium hydroxide / water / pH 14 / Inert atmosphere
2.1: triethylamine / acetone / 1 h / 0 °C / Inert atmosphere
3.1: sodium azide / water; acetone / 1 h / 0 °C / Inert atmosphere
3.2: Molecular sieve; atmospheric pressure short-path distillation; Inert atmosphere
4.1: ozone; Sudan III / dichloromethane / -78 °C
4.2: -78 °C
4.3: Reflux
5.1: N-Bromosuccinimide; ammonium acetate; water / acetone / 3 h / -78 - 20 °C / Inert atmosphere
With
N-Bromosuccinimide; sodium azide; ammonium acetate; water; ozone; silver nitrate; triethylamine; sodium hydroxide; Sudan III;
In
dichloromethane; water; acetone;
DOI:10.1021/jo2026228
