(2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

Base Information

Chemical Name:(2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate
CAS No.:904693-79-4
Molecular Formula:C₂₃H₂₇FO₇
Molecular Weight:434.462
Hs Code.:

Synonyms:(2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

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Chemical Property of (2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

Chemical Property:

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Technology Process of (2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

There total 1 articles about (2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoropent-4-en-2-yl 3-methylbenzoate

: 904693-79-4
(2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

: (2S,3R,4S,5S)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

Guidance literature:: With AD-mix-α; In water; tert-butyl alcohol; at 0 ℃;
DOI:10.1016/j.carres.2006.03.024

Reference yield: 75.0%

: 904693-79-4
(2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

: 904693-65-8
(2R,3R,4S,5S)-ethyl 6-(benzyloxy)-4-fluoro-2,3,5-trihydroxyhexanoate

Guidance literature:: With hydrogenchloride; In ethanol; for 24h; Heating;
DOI:10.1016/j.carres.2006.03.024

Reference yield:

: 904693-79-4
(2S,3R,4R,5R)-5-(ethoxycarbonyl)-1-(benzyloxy)-3-fluoro-4,5-dihydroxypentan-2-yl 3-methylbenzoate

: 904693-77-2
(3R,4R,5R,6S)-6-((benzyloxy)methyl)-5-fluoro-tetrahydro-3,4-dihydroxypyran-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / HCl / ethanol / 24 h / Heating

2: 90 percent / pyridinium toluenesulfonate / benzene / 5 h / Heating

With hydrogenchloride; pyridinium p-toluenesulfonate; In ethanol; benzene;
DOI:10.1016/j.carres.2006.03.024