Technology Process of C29H37F3N6O5
There total 7 articles about C29H37F3N6O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide;
at 70 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tert-butyl alcohol / 15 h / 23 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 23 °C
2.2: 48 h / -78 - 23 °C
3.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C
4.1: acetic acid / dichloromethane / 0.67 h / 23 °C
4.2: 15 h / 23 °C
5.1: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 23 °C
6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 18 h / 70 °C
With
lithium hydroxide; sodium hypochlorite; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium bromide;
In
tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tert-butyl alcohol / 15 h / 23 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 23 °C
2.2: 48 h / -78 - 23 °C
3.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C
4.1: acetic acid / dichloromethane / 0.67 h / 23 °C
4.2: 15 h / 23 °C
5.1: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 23 °C
6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 18 h / 70 °C
With
lithium hydroxide; sodium hypochlorite; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium bromide;
In
tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;