P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl

Base Information

Chemical Name:P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl
CAS No.:97764-40-4
Molecular Formula:C₂₀H₂₁BClOP
Molecular Weight:354.624
Hs Code.:

P(C<sub>6</sub>H<sub>5</sub>)2BH<sub>3</sub>CH<sub>2</sub>CHOHC<sub>6</sub>H<sub>4</sub>Cl

Synonyms:P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl

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Chemical Property of P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl

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Technology Process of P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl

There total 1 articles about P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 16940-66-2
sodium tetrahydroborate

: 97764-37-9
OP(C₆H₅)2CH₂CHOHC₆H₄Cl

: 97764-40-4
P(C₆H₅)2BH₃CH₂CHOHC₆H₄Cl

Guidance literature:: With CeCl₃*7H₂O; LiAlH₄; In tetrahydrofuran; CeCl3*7H2O was stirred in vac. at 140°C for 1 h, maintained at this temp. for 2 h; THF was added under N2; NaBH4 was added; stirring for1 h; phosphine oxide was added (ice bath), followed by LiAlH4 portionwise; stirring at room temp. for 2-15 h; diln. with benzene, pouring in ice/water/HCl; filtration through Celite; org. layer sepn.; extn. of aq. layer with C6H6; combined exts. was dried (Na2SO4) and evapd.; chromy. on silica gel; elem. anal.;
DOI:10.1021/ja00304a061