C₂₉H₂₃ClFNO₅S

Base Information

Chemical Name:C₂₉H₂₃ClFNO₅S
CAS No.:1273308-64-7
Molecular Formula:C₂₉H₂₃ClFNO₅S
Molecular Weight:552.023
Hs Code.:

C<sub>29</sub>H<sub>23</sub>ClFNO<sub>5</sub>S

Synonyms:C₂₉H₂₃ClFNO₅S

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Chemical Property of C₂₉H₂₃ClFNO₅S

Chemical Property:

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Technology Process of C₂₉H₂₃ClFNO₅S

There total 8 articles about C₂₉H₂₃ClFNO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1273308-06-7
methyl 4-(benzyloxycarbonylamino)-2-(4-chlorophenyl)thiophene-3-carboxylate

: 412018-61-2
C₉H₈ClFO

: 1273308-64-7
C₂₉H₂₃ClFNO₅S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; dmap; In dichloromethane; at 20 ℃; for 2.5h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1273308-64-7
C₂₉H₂₃ClFNO₅S

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

2: N-Bromosuccinimide / acetonitrile

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 1 h / 80 °C / Inert atmosphere

4: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; ethanol / 4 h / 760.05 Torr

5: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2.5 h / 20 °C

With N-Bromosuccinimide; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 69363-85-5
methyl 4-aminothiophene-3-carboxylate

: 1273308-64-7
C₂₉H₂₃ClFNO₅S

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

2: N-Bromosuccinimide / acetonitrile

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 1 h / 80 °C / Inert atmosphere

4: hydrogen / palladium 10% on activated carbon / dichloromethane; ethyl acetate; ethanol / 4 h / 760.05 Torr

5: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2.5 h / 20 °C

With N-Bromosuccinimide; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile;