3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

Base Information

Chemical Name:3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester
CAS No.:389087-54-1
Molecular Formula:C₇₆H₁₁₃FNO₁₃P
Molecular Weight:1298.7
Hs Code.:

3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

Synonyms:3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

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Chemical Property of 3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

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Technology Process of 3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

There total 4 articles about 3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.9%

: 389087-52-9
3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-2,4-dideoxy-6-O-diphenylphosphono-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-D-glycero-D-ido-octonic acid benzyl ester

: 389087-54-1
3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

Guidance literature:: With (diethylaminato)trifluorosulfur; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1246/bcsj.74.1661

Reference yield:

: 135561-34-1
benzyl <2-<(R)-3-(benzyloxy)tetradecanamido>-2-deoxy-3-O-<(R)-3-(tetradecanoyloxy)tetradecanoyl>-α-D-glucopyranosyl>acetate

: 389087-54-1
3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99.8 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 0.5 h / 20 °C

2: 95 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 4.5 h / 29 °C

3: 93.6 percent / aq. HCl / tetrahydrofuran / 7 h / 20 °C

4: 67.9 percent / (diethylaminato)trifluorosulfur / CH₂Cl₂ / 1.5 h / 20 °C

With hydrogenchloride; dmap; (diethylaminato)trifluorosulfur; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.74.1661

Reference yield:

: 389087-50-7
3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-8-O-t-butyldimethylsilyl-2,4-dideoxy-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-D-glycero-D-ido-octonic acid benzyl ester

: 389087-54-1
3,7-anhydro-4-[(R)-3-benzyloxytetradecanoylamino]-6-O-diphenylphosphono-8-fluoro-5-O-[(R)-3-(tetradecanoyloxy)tetradecanoyl]-2,4,8-trideoxy-D-glycero-D-ido-octonic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 4.5 h / 29 °C

2: 93.6 percent / aq. HCl / tetrahydrofuran / 7 h / 20 °C

3: 67.9 percent / (diethylaminato)trifluorosulfur / CH₂Cl₂ / 1.5 h / 20 °C

With hydrogenchloride; dmap; (diethylaminato)trifluorosulfur; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.74.1661