allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

Base Information

Chemical Name:allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside
CAS No.:195316-90-6
Molecular Formula:C₅₉H₅₁ClO₁₈
Molecular Weight:1083.5
Hs Code.:

Synonyms:allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

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Technology Process of allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

There total 6 articles about allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 127073-21-6
2,3,4-tri-O-benzoyl-6-O-chloroacetyl-α-D-glucopyranosyl chloride

: 195316-89-3
allyl 2,3,4-tri-O-benzoyl-α-D-galactopyranoside

: 195316-90-6
allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1080/07328309708006537

Reference yield: 70.0%

: 195316-92-8
2,3,4-tri-O-benzoyl-6-O-chloroacetyl-α-D-glucopyranosyl fluoride

: 195316-91-7
allyl 2,3,4-tri-O-benzoyl-6-O-trimethylsilyl-α-D-galactopyranoside

: 195316-90-6
allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1080/07328309708006537

Reference yield:

: 258854-17-0
1-O-Allyl 6-O-trityl-α-D-galactopyranoside

: 195316-90-6
allyl (2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 2 h / Ambient temperature

2: aq. AcOH / 6 h / 85 °C

3: 72 percent / AgOTf, sym-collidine, molecular sieves / CH₂Cl₂ / 1 h / 0 °C

With 2,4,6-trimethyl-pyridine; molecular sieve; silver trifluoromethanesulfonate; acetic acid; In dichloromethane;
DOI:10.1080/07328309708006537