(2-picolyl)diphenylborane dimer

Base Information

Chemical Name:(2-picolyl)diphenylborane dimer
CAS No.:1393596-95-6
Molecular Formula:C₃₆H₃₂B₂N₂
Molecular Weight:514.285
Hs Code.:

Synonyms:(2-picolyl)diphenylborane dimer

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Chemical Property of (2-picolyl)diphenylborane dimer

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Technology Process of (2-picolyl)diphenylborane dimer

There total 1 articles about (2-picolyl)diphenylborane dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 109-06-8
α-picoline

: 13471-36-8
methyl diphenylborinate

: 1393596-95-6
(2-picolyl)diphenylborane dimer

Guidance literature:: With n-butyllithium; BF₃*O(CH₂CH₃)2; In tetrahydrofuran; hexane; (inert atm.); addn. of butyllithium in hexane to picoline in THF at -78°C, keeping for 30 min, addn. of boron compd. in THF, warming to room temp. overnight, evapn., dissolving in CH2Cl2, addn. of BF3 etherate, keeping for 30 min; evapn., washing with ethanol, sonication in water, filtration, washing with ethanol, elem. anal.;
DOI:10.1039/c2ob25518a

Reference yield: 98.0%

: 1393596-95-6
(2-picolyl)diphenylborane dimer

: 75-05-8,26809-02-9
acetonitrile

: 1393597-13-1
Ph₂B(NHC(Me)CHC₅H₄N)

Guidance literature:: In toluene; (inert atm.); heating toluene soln. of boron compd. and 2 equiv. of CH3CN at 100°C for 12 h;
DOI:10.1039/c2ob25518a