Technology Process of C35H34N2O4
There total 2 articles about C35H34N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H33NO6;
With
diphenylphosphoranyl azide; triethylamine;
In
toluene;
at 20 ℃;
for 2h;
With
ethanol;
In
toluene;
at 70 ℃;
for 2h;
With
potassium hydroxide;
In
toluene;
for 3h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide; water / isopropyl alcohol / 3 h / Reflux
2.1: triethylamine; diphenylphosphoranyl azide / toluene / 2 h / 20 °C
2.2: 2 h / 70 °C
2.3: 3 h / Reflux
With
diphenylphosphoranyl azide; water; triethylamine; sodium hydroxide;
In
isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium nitrite / acetonitrile; water / 0.5 h / 0 - 5 °C
1.2: 6 h / 20 °C
2.1: n-butyllithium / toluene; hexane / 0.5 h / -50 °C
2.2: 3 h / 0 °C
3.1: ammonium formate / 5%-palladium/activated carbon / tetrahydrofuran / 8 h / 20 °C
With
hydrogenchloride; n-butyllithium; ammonium formate; sodium nitrite;
5%-palladium/activated carbon;
In
tetrahydrofuran; hexane; water; toluene; acetonitrile;