3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

Base Information

Chemical Name:3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide
CAS No.:1166859-56-8
Molecular Formula:C₂₀H₂₅NO₃SSi
Molecular Weight:387.575
Hs Code.:

Synonyms:3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

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Chemical Property of 3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

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Technology Process of 3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

There total 1 articles about 3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: C₂₀H₂₇NO₄SSi

: 1166859-56-8
3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Inert atmosphere; Reflux;
DOI:10.1021/jo900790k

Reference yield: 99.0%

: 1166859-56-8
3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

: 1166859-74-0
(S)-3-(3-{[(tert-butyldimethylsilyl)oxy]methyl}phenyl)-2,3-dihydrobenzo[d]isothiazole-1,1-dioxide

Guidance literature:: With C₄₀H₄₄IrN₆⁽¹⁺⁾*F₆P^(1-); ammonium formate; In water; N,N-dimethyl-formamide; at 60 ℃; for 4h; enantioselective reaction;
DOI:10.1039/c7cc04691j

Reference yield: 98.0%

: 1166859-56-8
3-[(t-butyldimethylsilyloxy)methyl]-phenyl-1,2-benzothiazole 1,1-dioxide

: 3-(3-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-2,3-dihydrobenzo[d]isothiazol-1,1-dioxide

Guidance literature:: With water; sodium acetate; cobalt(II) iodide; zinc; In acetonitrile; at 80 ℃; for 10h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201900636