rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

Base Information

Chemical Name:rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one
CAS No.:1604837-42-4
Molecular Formula:C₅₂H₅₉N₈O₅
Molecular Weight:876.091
Hs Code.:

Synonyms:rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

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Chemical Property of rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

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Technology Process of rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

There total 4 articles about rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.5%

: 6921-29-5
tripopargylamine

: 1604837-40-2
C₄₃H₅₀N₇O₅⁽¹⁺⁾

: 1604837-42-4
rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

Guidance literature:: With copper(l) iodide; In acetonitrile; at 20 ℃; for 3h;

Reference yield:

: rhodamine 101 piperazine amide

: 1604837-42-4
rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 3 h / 20 °C

2: copper(l) iodide / acetonitrile / 3 h / 20 °C

With copper(l) iodide; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; acetonitrile;

Reference yield:

: rhodamine 101

: 1604837-42-4
rhodamine 101 3-(2-(2-(4-((di(prop-2-yn-1-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)ethoxy)ethoxy)-1-(piperazin-1-yl)propan-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 2 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 20 °C / Cooling with ice

3: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 3 h / 20 °C

4: copper(l) iodide / acetonitrile / 3 h / 20 °C

With copper(l) iodide; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;