5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde

Base Information

Chemical Name:5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde
CAS No.:127426-60-2
Molecular Formula:C₁₁H₁₅NO₂
Molecular Weight:193.246
Hs Code.:
DSSTox Substance ID:DTXSID701241365
Nikkaji Number:J282.193A

Synonyms:DTXSID701241365;127426-60-2;5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde

Suppliers and Price of 5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:193.110278721
Heavy Atom Count:14
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=NOC(=C1C=O)C2CCCCC2

Technology Process of 5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde

There total 2 articles about 5-Cyclohexyl-3-methyl-4-isoxazolecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 127426-57-7
5-cyclohexyl-4-hydroxymethyl-3-methyl-isoxazol

: 127426-60-2
5-Cyclohexyl-3-methyl-isoxazol-4-carbaldehyd

Guidance literature:: With sodium dichromate; sulfuric acid; In dimethyl sulfoxide; 1. 50 deg C 2. 1h 70 deg C;
DOI:10.1055/s-1990-26789

Reference yield:

: 91247-88-0
5-cyclohexyl-3-methyl-isoxazol-4-carbonsaeure

: 127426-60-2
5-Cyclohexyl-3-methyl-isoxazol-4-carbaldehyd

Guidance literature:: Multi-step reaction with 2 steps

1: 1. Cl-CO₂Et, Et₃N 2. NaBH₄ / 1. THF, -10 deg C, 30 min 2. a. H₂O, 5-10 deg C b. 3h, room temperature

2: 71 percent / Na₂Cr₂O₇*2H₂O, H₂SO₄ / dimethylsulfoxide / 1. 50 deg C 2. 1h 70 deg C

With sodium tetrahydroborate; sodium dichromate; sulfuric acid; chloroformic acid ethyl ester; triethylamine; In dimethyl sulfoxide;
DOI:10.1055/s-1990-26789