1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

Base Information

Chemical Name:1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one
CAS No.:1446402-68-1
Molecular Formula:C₂₀H₂₁NO₃S
Molecular Weight:355.458
Hs Code.:

Synonyms:1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

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Chemical Property of 1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

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Technology Process of 1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

There total 4 articles about 1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 10579-60-9
1-(3,4-dihydroquinolin-1(2H)-yl)-2-methylprop-2-en-1-one

: 98-59-9
p-toluenesulfonyl chloride

: 1446402-68-1
1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

Guidance literature:: With 2,4,6-trimethyl-pyridine; 2C₂₉H₁₆NO₆S₂^(3-)*2C₃H₇NO*4Zn⁽²⁺⁾*O^(2-); In acetonitrile; at 20 ℃; for 24h; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1039/c8nj04151b

Reference yield: 60.0%

: 536-57-2
p-toluene sulfinic acid

: 10579-60-9
1-(3,4-dihydroquinolin-1(2H)-yl)-2-methylprop-2-en-1-one

: 1446402-68-1
1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

Guidance literature:: With tert.-butylhydroperoxide; eosin Y disodium salt; In water; at 20 ℃; for 6h; Irradiation;
DOI:10.1002/asia.201500498

Reference yield: 52.0%

: 10579-60-9
1-(3,4-dihydroquinolin-1(2H)-yl)-2-methylprop-2-en-1-one

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1446402-68-1
1-methyl-1-(tosylmethyl)-5,6-dihydro-1H-pyrrolo[3,2,1-ij]quinolin-2(4H)-one

Guidance literature:: With tert.-butylhydroperoxide; 18-crown-6 ether; potassium iodide; In water; at 80 ℃; for 2h; Green chemistry;
DOI:10.1021/jo401069d