C₄₅H₇₅N₃O₁₃

Base Information

Chemical Name:C₄₅H₇₅N₃O₁₃
CAS No.:497832-42-5
Molecular Formula:C₄₅H₇₅N₃O₁₃
Molecular Weight:866.103
Hs Code.:

C<sub>45</sub>H<sub>75</sub>N<sub>3</sub>O<sub>13</sub>

Synonyms:C₄₅H₇₅N₃O₁₃

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Chemical Property of C₄₅H₇₅N₃O₁₃

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Technology Process of C₄₅H₇₅N₃O₁₃

There total 8 articles about C₄₅H₇₅N₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 497832-02-7
C₄₃H₇₃N₃O₁₂

: 108-24-7
acetic anhydride

: 497832-42-5
C₄₅H₇₅N₃O₁₃

Guidance literature:: In acetone; at 20 ℃; for 6h;
DOI:10.1016/j.bmc.2012.08.007

Reference yield:

: 1395892-95-1
C₅₃H₈₂N₂O₁₆

: 497832-42-5
C₄₅H₇₅N₃O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: methanol / 18 h / Reflux

2.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C

3.1: lead(IV) tetraacetate / chloroform / 0.25 h / 0 °C

4.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C

5.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

7.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

7.2: 0.5 h / Reflux

8.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C

9.1: acetone / 6 h / 20 °C

With 1H-imidazole; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; ethanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.08.007

Reference yield:

: 79617-15-5
[10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-2-ethyl-3,4,9-trihydroxy-12-(5-hydroxy-4-methoxy-4,6-dimethyl-tetrahydro-pyran-2-yloxy)-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl]-carbamic acid benzyl ester

: 497832-42-5
C₄₅H₇₅N₃O₁₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C

2.1: lead(IV) tetraacetate / chloroform / 0.25 h / 0 °C

3.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C

4.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

5.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

6.2: 0.5 h / Reflux

7.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C

8.1: acetone / 6 h / 20 °C

With 1H-imidazole; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; ethanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.08.007