C₂₈H₃₈O₃Si

Base Information

• Chemical Name: C₂₈H₃₈O₃Si
• CAS No.: 950849-11-3
• Molecular Formula: C₂₈H₃₈O₃Si
• Molecular Weight: 450.693
• Mol file: 950849-11-3.mol

Synonyms:C₂₈H₃₈O₃Si

Chemical Property of C₂₈H₃₈O₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₃₈O₃Si

There total 7 articles about C₂₈H₃₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H42O4Si → C28H38O3Si (950849-11-3)

Guidance literature:

In tetrahydrofuran; water; acetic acid; at 35 ℃; for 96h;

DOI:10.1002/chem.200700302

Reference yield:

C30H42O4Si → C28H38O3Si (950849-11-3)

Guidance literature:

Multi-step reaction with 5 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 120 h / 20 °C

2: sodium methylate / methanol / 16 h / 20 °C

3: pyridine; Dess-Martin periodane / dichloromethane / 1 h / 20 °C

4: 0 °C

5: tetrahydrofuran; water; acetic acid / 96 h / 35 °C

With pyridine; dmap; sodium methylate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid;

DOI:10.1002/chem.200700302

Reference yield:

C28H40O3Si (950849-06-6) → C28H38O3Si (950849-11-3)

Guidance literature:

Multi-step reaction with 6 steps

1: pyridine; dmap / dichloromethane / 16 h / 20 °C

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 120 h / 20 °C

3: sodium methylate / methanol / 16 h / 20 °C

4: pyridine; Dess-Martin periodane / dichloromethane / 1 h / 20 °C

5: 0 °C

6: tetrahydrofuran; water; acetic acid / 96 h / 35 °C

With pyridine; dmap; sodium methylate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid;

DOI:10.1002/chem.200700302

upstream raw materials:

C₂₈H₄₀O₃Si

(1R,2R,3S,5S)-3-(tert-Butyl-diphenyl-silanyloxy)-5-((S)-1-methoxymethoxy-1-methyl-but-3-enyl)-2-methyl-cyclopentanecarbaldehyde

[(1R,2R,3S,5S)-3-(tert-Butyl-diphenyl-silanyloxy)-5-((S)-1-methoxymethoxy-1-methyl-but-3-enyl)-2-methyl-cyclopentyl]-methanol

tert-Butyl-[(1S,2R,3R,4S)-3-(4-methoxy-benzyloxymethyl)-4-(1-methoxymethoxy-1-methyl-but-3-enyl)-2-methyl-cyclopentyloxy]-diphenyl-silane

Downstream raw materials:

C₂₈H₄₀O₃Si