5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin

Base Information

• Chemical Name: 5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin
• CAS No.: 131443-56-6
• Molecular Formula: C₅₁H₃₅ClN₆O₃
• Molecular Weight: 815.33

Synonyms:5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin

Chemical Property of 5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin

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Technology Process of 5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin

There total 1 articles about 5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.2%

2,6-bis(chloromethyl)pyridine (3099-28-3) + 5-(3'-nitro-4'-hydroxyphenyl)-10,15,20-triphenylporphyrin (131443-55-5) → 2,5-di<2'-nitro-4'-(10,15,20-triphenyl-5-porphyrinyl)phenyl>oxymethylpyridine (136694-85-4) + 5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin (131443-56-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 8h;

DOI:10.1007/BF00480833

Reference yield: 91.0%

5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin (131443-56-6) + 2-hydroxynitrobenzene (88-75-5,78813-12-4) → 5-<3'-nitro-4'-<6''-methyleneoxy(2'''nitrophenyl)-2''-methyleneoxypyridyl>phenyl>-10,15,20-triphenylporphyrin (131443-57-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃;

DOI:10.1007/BF00480833

Reference yield: 83.4%

5-(3'-nitro-4'-hydroxyphenyl)-10,15,20-triphenylporphyrin (131443-55-5) + 5-<3'-nitro-4'-(6''-chloromethyl-2''-methyleneoxypyridyl)phenyl>-10,15,20-triphenylporphyrin (131443-56-6) → 2,5-di<2'-nitro-4'-(10,15,20-triphenyl-5-porphyrinyl)phenyl>oxymethylpyridine (136694-85-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃;

DOI:10.1007/BF00480833

upstream raw materials:

2,6-bis(chloromethyl)pyridine

5-(3'-nitro-4'-hydroxyphenyl)-10,15,20-triphenylporphyrin

Downstream raw materials:

2,5-di<2'-nitro-4'-(10,15,20-triphenyl-5-porphyrinyl)phenyl>oxymethylpyridine

5-<3'-nitro-4'-<6''-methyleneoxy(2'''nitrophenyl)-2''-methyleneoxypyridyl>phenyl>-10,15,20-triphenylporphyrin

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