(3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

Base Information

• Chemical Name: (3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione
• CAS No.: 144489-93-0
• Molecular Formula: C₂₇H₃₆N₂O₄
• Molecular Weight: 452.594

Synonyms:(3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

Chemical Property of (3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

Chemical Property:

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Technology Process of (3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione

There total 1 articles about (3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-Methyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-butyric acid 3-((S)-3-methyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-butyryloxy)-propyl ester (144406-53-1) → (3S,5R,6R,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione (169532-36-9) + (3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione (144489-93-0)

Guidance literature:

With methanesulfonic acid; zinc; In tetrahydrofuran; at 0 ℃; Product distribution; other solvents and temperature of reactions;

DOI:10.1021/jo00118a013

Reference yield:

(3S,5R,6S,8S)-3,8-Diisopropyl-5,6-diphenyl-1,10-dioxa-4,7-diaza-cyclotridecane-2,9-dione (144489-93-0) → meso-1,2-diphenyl-1,2-diaminoethane (951-87-1,5700-60-7,16635-95-3,29841-69-8,35132-20-8,107133-00-6)

Guidance literature:

With lead(IV) acetate; sodium hydroxide; Multistep reaction; 1.) EtOH, 40 deg C, 4 h, 2.) H₂O, 0 deg C, 2 h;

DOI:10.1021/jo00118a013

upstream raw materials:

(S)-3-Methyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-butyric acid 3-((S)-3-methyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-butyryloxy)-propyl ester

Downstream raw materials:

meso-1,2-diphenyl-1,2-diaminoethane

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