11-[4-(diethylamino)phenyl]-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

Base Information

Chemical Name:11-[4-(diethylamino)phenyl]-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one
CAS No.:298686-08-5
Molecular Formula:C₃₀H₃₃N₃O₂
Molecular Weight:467.611
Hs Code.:
Mol file:298686-08-5.mol

Synonyms:11-(4-diethylaminophenyl)-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydrodibenzo[b,e][1,4]diazepin-1-one

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Chemical Property of 11-[4-(diethylamino)phenyl]-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

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Technology Process of 11-[4-(diethylamino)phenyl]-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one

There total 3 articles about 11-[4-(diethylamino)phenyl]-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 3-(2-aminophenylamino)-5-(4-methoxyphenyl)-cyclohex-2-enone

: 120-21-8
4-Diethylaminobenzaldehyde

: 298686-08-5
11-(4-diethylaminophenyl)-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydrodibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: With hydrogenchloride; acetic acid; In ethanol; water; at 20 ℃;

Reference yield:

: 61888-41-3
3-chloro-5-(4-methoxyphenyl)-cyclohex-2-enone

: 298686-08-5
11-(4-diethylaminophenyl)-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydrodibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / ethanol / 48 h / Reflux

2: acetic acid; hydrogenchloride / ethanol; water / 20 °C

With hydrogenchloride; acetic acid; N-ethyl-N,N-diisopropylamine; In ethanol; water;

Reference yield:

: 1774-12-5
5-(4-methoxyphenyl)-1,3-cyclohexanedione

: 298686-08-5
11-(4-diethylaminophenyl)-3-(4-methoxyphenyl)-2,3,4,5,10,11-hexahydrodibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / ethanol / 48 h / Reflux

3: acetic acid; hydrogenchloride / ethanol; water / 20 °C

With hydrogenchloride; oxalyl dichloride; acetic acid; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In ethanol; dichloromethane; water;