1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene

Base Information

• Chemical Name: 1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene
• CAS No.: 76115-18-9
• Molecular Formula: C₂₈H₂₂O₂
• Molecular Weight: 390.481
• Mol file: 76115-18-9.mol

Synonyms:1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene

Chemical Property of 1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene

There total 2 articles about 1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(4'-acetoxyphenyl)-1,2,2-triphenylethane (76126-28-8) → 1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene (76115-18-9)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 10h; Heating;

Reference yield:

1-(4'-hydroxyphenyl)-1,2,2-triphenylethane (76119-87-4) → 1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene (76115-18-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / pyridine / 1) 1 h, 2) overnight, 30 deg C

2: 87 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 10 h / Heating

With pyridine; N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane;

Reference yield: 80.0%

1-(4'-acetoxyphenyl)-1,2,2-triphenylethylene (76115-18-9) → 1-(4'-hydroxyphenyl)-1,2,2-triphenylethylene (76115-06-5)

Guidance literature:

With sodium hydroxide; at 100 ℃; for 3.5h;

upstream raw materials:

1-(4'-acetoxyphenyl)-1,2,2-triphenylethane

1-(4'-hydroxyphenyl)-1,2,2-triphenylethane

Downstream raw materials:

1-(4'-hydroxyphenyl)-1,2,2-triphenylethylene

1-<4'-(β-diethylaminoethoxy)phenyl>-1,2,2-triphenylethylene

Refernces