methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Base Information

Chemical Name:methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate
CAS No.:339540-29-3
Molecular Formula:C₂₆H₃₂N₂O₈
Molecular Weight:500.549
Hs Code.:

Synonyms:methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Suppliers and Price of methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

There total 7 articles about methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)carbodiimido]-β-D-ribo-2-hexulofuranosonate

: 339540-29-3
methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 0.666667h;
DOI:10.1016/S0008-6215(02)00217-3

Reference yield:

: 30725-00-9
2,3-O-isopropylidene-D-ribonic-γ-lactone

: 339540-29-3
methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / NaH / dimethylformamide

2: 7.5 percent / P(NMe₂)3 / CH₂Cl₂

3: 54 percent / 4-chloroperoxybenzoic acid; hydroquinone / CH₂Cl₂ / 16 h / 20 °C

4: 95 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

5: tetrahydrofuran / 2 h / 24 °C

6: 904 mg / tetrahydrofuran / 72 h / 20 °C

7: 100 percent / HCl; water / tetrahydrofuran / 0.67 h / 20 °C

With hydrogenchloride; sodium azide; p-chloroperbenzoic acid; water; sodium hydride; hydroquinone; Hexamethylphosphorous triamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00217-3

Reference yield:

: 85846-80-6
5-O-benzyl-2,3-O-isopropylidene-D-ribono-1,4-lactone

: 339540-29-3
methyl 2,5-anhydro-6-O-benzyl-3,4-O-isopropylidene-2-[3-N-(4-methoxybenzyl)ureido]-β-D-ribo-2-hexulofuranosonate

Guidance literature:: Multi-step reaction with 6 steps

1: 7.5 percent / P(NMe₂)3 / CH₂Cl₂

2: 54 percent / 4-chloroperoxybenzoic acid; hydroquinone / CH₂Cl₂ / 16 h / 20 °C

3: 95 percent / NaN₃ / dimethylformamide / 5 h / 20 °C

4: tetrahydrofuran / 2 h / 24 °C

5: 904 mg / tetrahydrofuran / 72 h / 20 °C

6: 100 percent / HCl; water / tetrahydrofuran / 0.67 h / 20 °C

With hydrogenchloride; sodium azide; p-chloroperbenzoic acid; water; hydroquinone; Hexamethylphosphorous triamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00217-3