tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate

Base Information

• Chemical Name: tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate
• CAS No.: 1042690-70-9
• Molecular Formula: C₁₈H₂₆N₂O₄
• Molecular Weight: 334.415

Synonyms:tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate

Chemical Property of tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate

There total 1 articles about tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-(tert-butoxycarbonyl)-L-proline (15761-39-4,59433-50-0) + (2S)-2-phenylglycinol (20989-17-7) → tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate (1042690-70-9)

Guidance literature:

1-(tert-butoxycarbonyl)-L-proline; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 1h;

(2S)-2-phenylglycinol; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -15 - 20 ℃;

DOI:10.1515/hc-2017-0235

Reference yield:

tert-butyl (S)-2-[((S)-2-hydroxy-1-phenylethyl)carbamoyl]pyrrolidine-1-carboxylate (1042690-70-9) → C18H24N2O3 (1042690-63-0)

Guidance literature:

With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at -20 ℃;

DOI:10.1016/j.bmcl.2009.09.078

upstream raw materials:

1-(tert-butoxycarbonyl)-L-proline

(2S)-2-phenylglycinol

Downstream raw materials:

C₁₈H₂₄N₂O₃

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