2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide

Base Information

Chemical Name:2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide
CAS No.:81236-00-2
Molecular Formula:C₂₄H₂₈N₂O₅
Molecular Weight:424.497
Hs Code.:

Synonyms:2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide

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Technology Process of 2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide

There total 6 articles about 2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 81235-88-3
2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-methoxyethyl)-3-butenamide

: 81236-00-2
2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide

Guidance literature:: With Trimethyl(methylthio)silane; tetra-(n-butyl)ammonium iodide; zinc(II) iodide; In 1,2-dichloro-ethane; at 80 ℃; for 1.5h;
DOI:10.1139/v83-091

Reference yield:

: 857975-91-8
ethyl 3-(2-mewthoxyethyl)-3-methylglycidate

: 81236-00-2
2-acetoxy-N-benzyl-N-(2-benzylamino-2-oxoethyl)-3-(2-hydroxyethyl)-3-butenamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1) Ac₂O, H₂SO₄, 2) HCl / 2) EtOH

2: 25percent aq. NaOH

4: ClCOCOCl

6: MeSSiMe₃

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; Trimethyl(methylthio)silane; sulfuric acid; acetic anhydride;
DOI:10.1039/c39810001126