C₃₈H₃₆N₂O₉

Base Information

Chemical Name:C₃₈H₃₆N₂O₉
CAS No.:1532519-04-2
Molecular Formula:C₃₈H₃₆N₂O₉
Molecular Weight:664.712
Hs Code.:

C<sub>38</sub>H<sub>36</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₈H₃₆N₂O₉

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Chemical Property of C₃₈H₃₆N₂O₉

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Technology Process of C₃₈H₃₆N₂O₉

There total 8 articles about C₃₈H₃₆N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1532519-02-0
di-tert-butyl (2S,3S,4S)-4-(5-(3-aminopropyl)-2-methoxyphenyl)-3-(2-(tert-butoxy)-2-oxoethyl)pyrrolidine-1,2-dicarboxylate

: 1532519-03-1
C₂₃H₁₈O₆

: 1532519-04-2
C₃₈H₃₆N₂O₉

Guidance literature:: di-tert-butyl (2S,3S,4S)-4-(5-(3-aminopropyl)-2-methoxyphenyl)-3-(2-(tert-butoxy)-2-oxoethyl)pyrrolidine-1,2-dicarboxylate; C₂₃H₁₈O₆; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ol403434e

Reference yield:

: 1532518-98-1
di-tert-butyl (2R,3S,4S)-3-(2-(tert-butoxy)-2-oxoethyl)-4-(2-methoxyphenyl)pyrrolidine-1,2-dicarboxylate

: 1532519-04-2
C₃₈H₃₆N₂O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butylate; tert-butyl alcohol / benzene / 1 h / 0 - 20 °C

2.1: iodine; silver nitrate / acetonitrile / 2 h / 20 - 60 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / acetonitrile / 1 h / 20 °C / Sonication

4.1: triethylamine / dichloromethane / 2 h / 0 °C

5.1: sodium azide; sodium iodide / N,N-dimethyl-formamide / 1 h / 20 - 60 °C

6.1: hydrogen; palladium on activated charcoal / methanol / 3 h / 20 °C

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

7.2: 3 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; palladium on activated charcoal; potassium tert-butylate; hydrogen; iodine; benzotriazol-1-ol; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide; tert-butyl alcohol; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; benzene; 3.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol403434e

Reference yield:

: 1532518-97-0
C₂₂H₃₃NO₅

: 1532519-04-2
C₃₈H₃₆N₂O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 2 h / 20 °C

2.1: potassium tert-butylate; tert-butyl alcohol / benzene / 1 h / 0 - 20 °C

3.1: iodine; silver nitrate / acetonitrile / 2 h / 20 - 60 °C

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / acetonitrile / 1 h / 20 °C / Sonication

5.1: triethylamine / dichloromethane / 2 h / 0 °C

6.1: sodium azide; sodium iodide / N,N-dimethyl-formamide / 1 h / 20 - 60 °C

7.1: hydrogen; palladium on activated charcoal / methanol / 3 h / 20 °C

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

8.2: 3 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; palladium on activated charcoal; potassium tert-butylate; hydrogen; iodine; benzotriazol-1-ol; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide; tert-butyl alcohol; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; benzene; 4.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol403434e