C₁₈H₃₀O

Base Information

• Chemical Name: C₁₈H₃₀O
• CAS No.: 1428957-07-6
• Molecular Formula: C₁₈H₃₀O
• Molecular Weight: 262.436
• Mol file: 1428957-07-6.mol

Synonyms:C₁₈H₃₀O

Chemical Property of C₁₈H₃₀O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₃₀O

There total 12 articles about C₁₈H₃₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C20H32O2 (1428957-06-5) → C18H30O (1428957-07-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → C18H30O (1428957-07-6)

Guidance literature:

Multi-step reaction with 12 steps

1.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

1.2: -40 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

3.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

4.1: sodium ethanolate / ethanol / 0 °C

4.2: 16 h / 0 - 20 °C

5.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

6.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

6.2: -40 - 20 °C

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

8.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

9.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere

9.2: 16 h / 0 - 20 °C

10.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

11.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

11.2: -40 - 20 °C

12.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;

Reference yield:

ethyl cyclohexylideneacetate (1552-92-7) → C18H30O (1428957-07-6)

Guidance literature:

Multi-step reaction with 11 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

2.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

3.1: sodium ethanolate / ethanol / 0 °C

3.2: 16 h / 0 - 20 °C

4.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

5.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

5.2: -40 - 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

7.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

8.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere

8.2: 16 h / 0 - 20 °C

9.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

10.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

10.2: -40 - 20 °C

11.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;

upstream raw materials:

cyclohexanone

ethyl cyclohexylideneacetate

2-cyclohexylidene ethanol

(2-bromoethylidene)cyclohexane

Downstream raw materials:

C₁₈H₂₉Br

C₂₄H₃₈O₃

C₂₁H₃₄O

C₂₅H₄₀O₂