(3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

Base Information

Chemical Name:(3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine
CAS No.:1097198-47-4
Molecular Formula:C₃₁H₄₄N₂O₆Si
Molecular Weight:568.786
Hs Code.:

Synonyms:(3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

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Chemical Property of (3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

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Technology Process of (3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

There total 1 articles about (3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 109838-85-9
(2R)-2,5-dihydro-2-isopropyl-3,6-dimethoxypyrazine

: (2R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-[1,3]dioxane-4-carbaldehyde

: 1097198-47-4
(3S,6R,1'R,2'S,3'R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

: 1097198-50-9
(3S,6R)-3-(3-tert-butyldiphenylsilyloxy-1-hydoxy-2,4-ethylidenedioxybutyl)-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

Guidance literature:: (2R)-2,5-dihydro-2-isopropyl-3,6-dimethoxypyrazine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

With tin(ll) chloride; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

(2R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-[1,3]dioxane-4-carbaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 4h;
DOI:10.1039/b810878a